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41.
Rapid and Nondestructive Identification of Polytypism and Stacking Sequences in Few‐Layer Molybdenum Diselenide by Raman Spectroscopy 下载免费PDF全文
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Usman Abdulfatai Adamu Uzairu Sani Uba Gideon Adamu Shallangwa 《Egyptian Journal of Petroleum》2019,28(2):241-245
Quantitative structure-properties relationship (QSPR) method was used to design some novel antioxidant lubricant additives, while molecular dynamics simulations were used to calculate their dynamic binding energies on steel and to hydrogen-containing DLC (a-C: H) crystal surfaces. 29 synthesized antioxidant lubricant additives were collected from literature and geometrically optimized by Spartan’14 version 1.1.2 software while Genetic Function Algorithm (GFA) method of the material studio version 8.0 software was used to build the predictive QSPR model. Four novel antioxidant lubricant additives were successfully designed out of which E)-3-(4-((3-amino-4-methylphenyl)diazenyl)-5-hydroxy-4H-pyrazol-3-yl)-2-argio-6,7-difluoroquinazolin-4(3H)-one with excellent property of 3.531295 (KOH/g) was found to be better than the one reported by other researchers. The dynamic binding energy results revealed that one of the designed additives was excellently bound to steel (?1120.11 kcal/mol) and to hydrogen-containing DLC (a-C: H) crystals surface (7814.156 kcal/mol) surfaces than its co-additives. This investigation shows that the entire studied antioxidant lubricant additive was found to be better bound to the steel surface than hydrogen-containing DLC (a-C: H) crystals surface. This study will help in synthesizing novel anti-oxidant lubricant additives with better additive properties that will slow the tendency of oil to oxidize and will not possess a threat to the environment as the structures do not contain zinc and phosphorus that could limit the operation of the catalytic converter in the exhaust pipe. 相似文献
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Syed Altan Haider Muhammad Sajid Saeed Iqbal 《International Journal of Hydrogen Energy》2021,46(2):1671-1681
The focus of this study is the use of Machine Learning methods to forecast Solar Hydrogen production potential for the Islamabad region of Pakistan. For this purpose, we chose a Photovoltaic-Electrolytic (PV-E) system to forecast electricity and, hence, hydrogen production. The weather data used for forecasting and simulation were recorded with precise meteorological instruments stationed in Islamabad, over the course of 13 and a half months. Out of the three tested algorithms, Prophet performs the best with Mean Absolute Percentage Error of 3.7%, forecasting a daily average Hydrogen production of 93.3 × 103 kg/Km2. Although, the forecast in this study is made for the month of August and September, during which the local season moves towards winter, this study demonstrates solar hydrogen production, as a green energy source, has a tremendous potential in this region. 相似文献
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Zahid Hussain Shar Mary T. Fletcher Gul Amer Sumbal Syed Tufail Hussain Sherazi Cindy Giles Muhammad Iqbal Bhanger 《Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment》2016,33(5):849-860
This work reports the application of banana peel as a novel bioadsorbent for in vitro removal of five mycotoxins (aflatoxins (AFB1, AFB2, AFG1, AFG2) and ochratoxin A). The effect of operational parameters including initial pH, adsorbent dose, contact time and temperature were studied in batch adsorption experiments. Scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR) and point of zero charge (pHpzc) analysis were used to characterise the adsorbent material. Aflatoxins’ adsorption equilibrium was achieved in 15 min, with highest adsorption at alkaline pH (6–8), while ochratoxin has not shown any significant adsorption due to surface charge repulsion. The experimental equilibrium data were tested by Langmuir, Freundlich and Hill isotherms. The Langmuir isotherm was found to be the best fitted model for aflatoxins, and the maximum monolayer coverage (Q0) was determined to be 8.4, 9.5, 0.4 and 1.1 ng mg?1 for AFB1, AFB2, AFG1 and AFG2 respectively. Thermodynamic parameters including changes in free energy (ΔG), enthalpy (ΔH) and entropy (ΔS) were determined for the four aflatoxins. Free energy change and enthalpy change demonstrated that the adsorption process was exothermic and spontaneous. Adsorption and desorption study at different pH further demonstrated that the sorption of toxins was strong enough to sustain pH changes that would be experienced in the gastrointestinal tract. This study suggests that biosorption of aflatoxins by dried banana peel may be an effective low-cost decontamination method for incorporation in animal feed diets. 相似文献
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Muhammad Ashraf Bajeer Muhammad Ali Mallah Syed Tufail Hussain Sherazi Muhammad Iqbal Bhanger Shafi Muhammad Nizamani 《Polycyclic Aromatic Compounds》2016,36(3):229-241
This study concerns the investigation of dissipation, adsorption, and degradation of triazophos in different soils from Pakistan. These processes help in the disappearance of pesticide from the environment. Gas chromatography was used for dissipation and adsorption analysis while for degradation study mass spectrometer was used in addition of gas chromatography (GC-MS). The dissipation rate of triazophos in three different soils was 90% over 30 days with average half-life of 9.059 days. From dissipation study it was inferred that rate is variable in each soil due to climatic changes, soil nature and soil-pesticide interactions. Adsorption experiment has revealed that the adsorption of this pesticide to soil follows the pseudo first order kinetic model with rate constant value of 0.479/h and Freundlich isotherm with adsorption capacity of 1.832 mol/g. Degradation study has displayed two major metabolites, one is phosphorothioic acid, S-[2-[(1-cyano-1-methylethyl) amino]-2-oxoethyl] O,O-diethyl ester at retention time of 9.136 and the other is sulfotep at 14.304 min. The leaching potential of triazophos was also calculated from its half-life and organic carbon content present in soil which was 1.688 representing it as non leacher pesticide. 相似文献
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S.S.Batool Z.Imran M.Israr Qadir M.Usman H.Jamil M.A Rafiq M.M.Hassan M.Willander 《材料科学技术学报》2013,29(5):411-414
The effect of metal(Ti,Ni,and Au) electrodes on humidity sensing properties of electrospun TiO2 nanofibers was investigated in this work.The devices were fabricated by evaporating metal contacts on SiO2 layer thermally grown on silicon substrate.The separation between the electrodes was 90μm for all sensors.The sensors were tested from 40%to 90%relative humidity(RH) by AC electrical characterization at room temperature. When sensors are switched between 40%and 90%RH,the corresponding response and recovery time are 3 s and 5 s for Ti-electrode sensor,4 s and 7 s for Ni-electrode sensor,and 7 s and 13 s for Au-electrode sensor.The hysteresis was 3%,5%and 15%for Ti-,Ni-,and Au-electrode sensor,respectively.The sensitivity of Ti,Ni,and Au-electrode sensors are 7.53 MΩ/%RH,5.29 MΩ/%RH and 4.01 MΩ/%RH respectively at 100 Hz.Therefore Ti-electrode sensor is found to have linear response,fast response and recovery time and higher sensitivity as compared with those of Ni- and Au-electrode sensors.Comparison of humidity sensing properties of sensors with different electrode material may propose a compelling route for designing and optimizing humidity sensors. 相似文献